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Nuclear Magnetic Resonance Spectroscopy

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ISBN: 9783038429937 9783038429944 Year: Pages: X, 298 Language: englisch
Publisher: MDPI - Multidisciplinary Digital Publishing Institute
Subject: Chemistry (General)
Added to DOAB on : 2018-08-21 14:42:20
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Nuclear Magnetic Resonance (NMR) spectroscopy is a nondestructive technique that can be used to characterize a wide variety of systems. Sustained development of both methodology and instrumentation have allowed NMR to evolve as a powerful technology, with applications in pure sciences, medicine, drug development, and important branches of industry. NMR provides precise structural information down to each atom and bond in a molecule, and is the only method for the determination of structures of molecules in a solution. This book compiles a series of articles describing the application of NMR in a variety of interesting scientific challenges. The articles illustrate the versatility and flexibility of NMR.

Carbon Fibers

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ISBN: 9783906980690 9783906980706 Year: Pages: 192 DOI: 10.3390/books978-3-906980-70-6 Language: English
Publisher: MDPI - Multidisciplinary Digital Publishing Institute
Added to DOAB on : 2015-10-22 06:30:12
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Remarkably, truly novel structures are still being found for materials made of a single element: carbon. Perhaps there is a ‘revolution’ in carbon-only materials. Indeed, recently, two Nobel prizes were awarded for new forms of carbon: for fullerenes in 1996, and for graphene in 2010. And the magic and beauty of carbon nanotubes has held the attention of the scientific world for more than a decade. Yet, there is still more to discover and to explain. In this Special Issue, the focus is on just one area of carbon research: fibers. Even given this relatively narrow focus there is a diversity of research that is both compelling and frustrating. Compelling as it demonstrates the vitality of the subject, and frustrating as it makes it difficult to organize. The topics covered include new fiber fabrication protocols, the mechanical behavior of fiber reinforced polymers, new techniques to study the microstructure of fiber containing composites, new uses of fiber structures, the use of carbon fibers as catalyst supports, and studies regarding the difficulties of machining fiber structures for inclusion in complex structures.

Nanofibres: Friend or Foe?

ISBN: 9783038422785 9783038422792 Year: Pages: XII, 178 Language: English
Publisher: MDPI - Multidisciplinary Digital Publishing Institute
Subject: Chemistry (General)
Added to DOAB on : 2016-12-19 09:28:28
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Nanofibers, particularly those of a carbonaceous content, have received increased interest in the past two decades due to their outstanding physico-chemical characteristics and their possibility to form and contribute towards a plethora of potentially advantageous materials for consumer, industrial and medical applications. Despite this, and together with the numerous research studies and published articles that have sought to investigate these aspects, the potential impact of CNTs is still not understood. Whether or not nanofibers may be able to provide a sophisticated alternative to conventional materials is still debatable, whilst their effects upon both environmental and human health are highly equivocal. How nanofibers are conceived can determine how they may interact with different environments, such as the human body. Understanding each key step of the synthesis and production of nanofibers to their use within potential applications is therefore essential in gaining an insight into how they may be perceived by any biological system and environment. Thus, obtaining such information will enable all scientific communities to begin to realize the potential advantages posed by nanofibers. The aim of this Special Issue therefore, was to provide a collective overview of nanofibers; ‘from synthesis to application’. The Issue particularly focuses upon carbon-based nanofibers, but also highlights alternative nanofiber types. Emphasis is given holistically, with articles discussing the production routes of nanofibers, their plight during their life-cycle (origin to applied form and effects over time), as well as how nanofibers could either incite conflict, or provide aid to human and environmental health.

Trends in Microextraction Techniques for Sample Preparation

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ISBN: 9783038427056 9783038427063 Year: Pages: 246 Language: English
Publisher: MDPI - Multidisciplinary Digital Publishing Institute
Subject: Chemistry (General)
Added to DOAB on : 2018-01-24 14:09:38
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Micro-extraction techniques in sample preparation are gaining interest among analytical chemists as they comply with green analytical chemistry demands and ensure environmental protection and public safety. Savings in cost and time are considered as valuable benefits by using novel micro-extraction approaches in sample handling. Selectivity, sensitivity and lower detection limits are also included among the performance characteristics required to meet the legislation criteria.The target of this special issue is to present the state of art in microextraction sample preparation techniques. Modern, simple and efficient methods for preconcentration and separation are described for different analytes isolated from various matrices.

Trends in Microextraction Techniques for Sample Preparation

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ISBN: 97830384270569783038427063 Year: Pages: 246 Language: English
Publisher: MDPI - Multidisciplinary Digital Publishing Institute
Subject: Chemistry (General)
Added to DOAB on : 2018-01-31 12:42:43
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The Molecular Aspect of Natural Secondary Metabolite Products in Health and Disease

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ISBN: 9783038971764 9783038971771 Year: Pages: 226 DOI: 10.3390/books978-3-03897-177-1 Language: English
Publisher: MDPI - Multidisciplinary Digital Publishing Institute
Subject: Anthropology --- Social and Public Welfare --- Biology
Added to DOAB on : 2018-09-19 09:01:21
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ca. 200 words; this text will present the book in all promotional forms (e.g. flyers). Please describe the book in straightforward and consumer-friendly terms.[Natural secondary metabolite products, which are isolated from plants, animals, microorganisms, etc., are classified as polyketides, isoprenoids, steroids, aromatics, alkaloids, etc. Their chemical diversity and variety of biological activities have attracted the attention of chemists, biochemists, biologists, etc. This Special Issue on "The Molecular Aspect of Natural Secondary Metabolite Products in Health and Disease" is intended to offer biological active natural products as candidates and/or leads for pharmaceuticals, dietary supplements, functional foods, cosmetics, food additives, etc. The research fields of this Special Issue include natural products chemistry, phytochemistry, pharmacognosy, food chemistry, bioorganic synthetic chemistry, molecular pharmacology, molecular nutritional sciences, and other related research fields of bioactive natural secondary metabolite products. Original research and review articles on all topics in these research fields are invited. I look forward to receiving many submissions from outstanding expert on these research fields.

Biological Activity of Natural Secondary Metabolite Products

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ISBN: 9783038971740 9783038971757 Year: Pages: 466 DOI: 10.3390/books978-3-03897-175-7 Language: English
Publisher: MDPI - Multidisciplinary Digital Publishing Institute
Subject: Anthropology --- Biology --- Social and Public Welfare
Added to DOAB on : 2018-09-20 12:02:36
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ca. 200 words; this text will present the book in all promotional forms (e.g. flyers). Please describe the book in straightforward and consumer-friendly terms.[Natural secondary metabolite products, which are isolated from plants, animals, microorganisms, etc., are classified as polyketides, isoprenoids, aromatics (phenylpropanoids), alkaloids, etc. Their chemical diversity and variety of biological activities have attracted the attention of chemists, biochemists, biologists, etc. The Special Issue on "Biological Activity of Natural Secondary Metabolite Products" is intended to offer biological active natural products as candidates and/or leads for pharmaceuticals, dietary supplements, functional foods, cosmetics, food additives, etc. The research fields of this Special Issue include natural products chemistry, phytochemistry, pharmacognosy, food chemistry, bioorganic synthetic chemistry, chemical biology, molecular biology, molecular pharmacology, and other related research fields of bioactive natural secondary metabolite products. Original research and review articles on all topics in these research fields are invited. I am looking forward to receiving many submissions from outstanding experts in these research fields.]

Current Aspects of Radiopharmaceutical Chemistry

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ISBN: 9783038971627 9783038971634 Year: Pages: 216 DOI: 10.3390/books978-3-03897-163-4 Language: English
Publisher: MDPI - Multidisciplinary Digital Publishing Institute
Subject: Internal medicine --- Chemistry (General)
Added to DOAB on : 2018-09-19 11:46:43
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Positron emission tomography (PET) and single-photon emission computed tomography (SPECT) are in vivo molecular imaging techniques which are widely used in nuclear medicine for the diagnosis and treatment follow-up of many major diseases. They use biomolecules as probes, which are labeled with radionuclides of short half-lives, synthesized prior to the imaging studies. These probes are called radiopharmaceuticals. Their design and development require a rather interdisciplinary process involving many different disciplines of natural and health sciences. In addition to their diagnostic and therapeutic purposes in the field of nuclear medicine, radiopharmaceuticals provide powerful tools for in vivo pharmacology during the process of pre-clinical drug development to identify new drug targets, investigate the pathophysiology of diseases, discover potential drug candidates, and evaluate the pharmacokinetics and pharmacodynamics of drugs in vivo. Furthermore, they allow molecular imaging studies in various small-animal models of disease, including genetically engineered animals. The current collection of articles provides unique examples covering all major aspects in the field.

Biomass Chars: Elaboration, Characterization and Applications

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ISBN: 9783038426905 9783038426912 Year: Pages: 220 DOI: 10.3390/books978-3-03842-691-2 Language: English
Publisher: MDPI - Multidisciplinary Digital Publishing Institute
Subject: Chemistry (General)
Added to DOAB on : 2018-01-12 11:37:17
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Thermochemical conversion processes convert biomass into gaseous, liquid and solid products named, syngas, bio-oil and char, respectively. Syngas and bio-oil are considered as alternative biofuels to fossil fuels and wide investigations are implemented currently on their production, purification, modification, and applications. Biomass chars have receiving an increasing attention since they lead to carbon sequestration, reduction of the amount of carbon rejected into the atmosphere and represent an friendly carbon source for numerous applications. In particular, biomass chars could be an efficient materials for energy production, syngas production and upgrading, water and air pollutants removal, soil amendment, fuel cells and supercapacitors development, and gas storage. Improving the knowledge of biomass chars elaboration techniques such as pyrolysis, gasification and hydrothermal carbonization is essential to determine the optimal production strategies for their economic viability. Furthermore, the characterization of the physicochemical, textural, structural and surface chemistry properties of the derived chars guide the selection of the suitable recovery processes in order to maximize their utility and therefore the benefits for the environment as well as for industries and agriculture.

Design and Engineering of Microreactor and Smart-Scaled Flow Processes

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ISBN: 9783038420385 9783038420392 Year: Pages: 252 DOI: 10.3390/books978-3-03842-039-2 Language: English
Publisher: MDPI - Multidisciplinary Digital Publishing Institute
Added to DOAB on : 2015-10-22 07:00:06
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Microreactors are small devices with sub-millimeter internals which have superb mass and heat transfer. Initially, they were used for reactions with very high demands on the latter, e.g. very exothermic reactions, gas-liquid reactions with interfacial transport issues, reactions with very fast kinetics which demands even faster mixing, and more. In this way, the processing window was opened widely and, also due to the minute volumes only present in the reaction zone, safe processing under otherwise hazardous conditions was enabled. This includes processing of reactions which are prone to thermal runaway and in the explosive regime. Scale-up of promising reactions and products which was hindered with conventional technology is now possible using the new equipment. This has widened the process development possibilities in chemical industry.In the last years, micro process technology was not only used for the very problematic synthetic issues which formerly had a dead-end position in industry’s process development. Rather, the scope of chemical reactions to be processed in microreactors was considerably widened by exploring new process conditions with regard to temperature, pressure, concentration, solvents, and more. This is commonly referred to as flow chemistry. This allowed to reduce the processing time-scale for many reactions to the minute range or even below which fits well to the residence times of microreactors. In addition, the process integration of several reactions in one flow to a multi-step synthesis has opened a new door in molecular diversity as well as system and process complexity. The same holds for the combination of reactions and separations in micro-flow. To achieve throughputs relevant for industrial production, smart scale-out to milli-flow units has established and supplemented the num­bering-up concept (parallelization of microchannels/-reactors operated under equal conditions).New innovations and enabling technologies need anyhow evaluation and benchmarking with conventional technology on the full-system level. Yet, microreactor technology has in the last years deepened so much into process intensification on a holistic scale that the focus increasingly is given towards the process dimension—to process design and automation, real-case applications, cost analysis, life-cycle assessment, and more. The impact on cost competitiveness and sustainability becomes well assessed.Facing this very recent scientific achievement, the special issue “Design and Engineering of Microreactor and Smart-Scaled Flow Processes” of the journal Processes aims to cover recent advances in the development of microreactor and smart-scaled flow processes towards the process level — in the sense as given above.

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